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Henley's Twentieth Century Formulas, Recipes and Processes · Gardner Dexter Hiscox — chapter 3 of 563 · ~1,078 words · public domain

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«To Prevent Glue from Cracking.»—To prevent glue from cracking, which frequently occurs when glued articles are {11} exposed to the heat of a stove, a little chloride of potassium is added. This prevents the glue from becoming dry enough to crack. Glue thus treated will adhere to glass, metals, etc., and may also be used for pasting on labels.

«Preventing the Putrefaction of Strong Glues.»—The fatty matter always existing in small quantity in sheets of ordinary glue affects the adhesive properties and facilitates the development of bacteria, and consequently putrefaction and decomposition. These inconveniences are remedied by adding a small quantity of caustic soda to the dissolved glue. The soda prevents decomposition absolutely; with the fatty matter it forms a hard soap which renders it harmless.

«Liquid Glues.»—

I.—Glue 3 ounces Gelatin 3 ounces Acetic acid 4 ounces Water 2 ounces Alum 30 grains

Heat together for 6 hours, skim, and add:

II.—Alcohol 1 fluid ounce Brown glue, No. 2. 2 pounds Sodium carbonate 11 ounces Water 3 1⁠/⁠2 pints Oil of clove 160 minims

Dissolve the soda in the water, pour the solution over the dry glue, let stand over night or till thoroughly soaked and swelled, then heat carefully on a water bath until dissolved. When nearly cold stir in the oil of cloves.

By using white glue, a finer article, fit for fancy work, may be made.

III.—Dissolve by heating 60 parts of borax in 420 parts of water, add 480 parts dextrin (pale yellow) and 50 parts of glucose and heat carefully with continued stirring, to complete solution; replace the evaporated water and pour through flannel.

The glue made in this way remains clear quite a long time, and possesses great adhesive power; it also dries very quickly, but upon careless and extended heating above 90° C. (194° F.), it is apt to turn brown and brittle.

IV.—Pour 50 parts of warm (not hot) water over 50 parts of Cologne glue and allow to soak over night. Next day the swelled glue is dissolved with moderate heat, and if still too thick, a little more water is added. When this is done, add from 2 1⁠/⁠2 to 3 parts of crude nitric acid, stir well, and fill the liquid glue in well-corked bottles. This is a good liquid steam glue.

V.—Soak 1 pound of good glue in a quart of water for a few hours, then melt the glue by heating it, together with the unabsorbed water, then stir in 1⁠/⁠4 pound dry white lead, and when that is well mixed pour in 4 fluidounces of alcohol and continue the boiling 5 minutes longer.

VI.—Soak 1 pound of good glue in 1 1⁠/⁠2 pints of cold water for 5 hours, then add 3 ounces of zinc sulphate and 2 fluidounces of hydrochloric acid, and keep the mixture heated for 10 or 12 hours at 175° to 190° F. The glue remains liquid and may be used for sticking a variety of materials.

VII.—A very inexpensive liquid glue may be prepared by first soaking and then dissolving gelatin in twice its own weight of water at a very gentle heat; then add glacial acetic acid in weight equal to the weight of the dry gelatin. It should be remembered, however, that all acid glues are not generally applicable.

VIII.—Glue 200 parts Dilute acetic acid 400 parts

Dissolve by the aid of heat and add:

Alcohol 25 parts Alum 5 parts

IX.—Glue 5 parts Calcium chloride 1 part Water 1 part

X.—Sugar of lead 1 1⁠/⁠2 drachms Alum 1 1⁠/⁠2 drachms Gum arabic 2 1⁠/⁠2 drachms Wheat flour 1 av. lb. Water, q. s.

Dissolve the gum in 2 quarts of warm water; when cold mix in the flour, and add the sugar of lead and alum dissolved in water; heat the whole over a slow fire until it shows signs of ebullition. Let it cool, and add enough gum water to bring it to the proper consistence.

XI.—Dilute 1 part of official phosphoric acid with 2 parts of water and neutralize the solution with carbonate of ammonium. Add to the liquid an equal quantity of water, warm it on a water bath, and dissolve in it sufficient glue to form a thick syrupy liquid. Keep in well-stoppered bottles.

XII.—Dissolve 3 parts of glue in small pieces in 12 to 15 of saccharate of lime. By heating, the glue dissolves rapidly and remains liquid, when cold, without loss of adhesive power. Any desirable consistence can be secured by varying the amount of saccharate of lime. Thick glue retains its muddy color, while a thin solution becomes clear on standing.

The saccharate of lime is prepared by {12} dissolving 1 part of sugar in 3 parts of water, and after adding 1⁠/⁠4 part of the weight of the sugar of slaked lime, heating the whole from 149° to 185° F., allowing it to macerate for several days, shaking it frequently. The solution, which has the properties of mucilage, is then decanted from the sediment.

XIII.—In a solution of borax in water soak a good quantity of glue until it has thoroughly imbibed the liquid. Pour off the surplus solution and then put on the water bath and melt the glue. Cool down until the glue begins to set, then add, drop by drop, with agitation, enough acetic acid to check the tendency to solidification. If, after becoming quite cold, there is still a tendency to solidification, add a few drops more of the acid. The liquid should be of the consistence of ordinary mucilage at all times.

XIV.—Gelatin 100 parts Cabinetmakers’ glue 100 parts Alcohol 25 parts Alum 2 parts Acetic acid, 20 per cent 800 parts

Soak the gelatin and glue with the acetic acid and heat on a water bath until fluid; then add the alum and alcohol.

XV.—Glue 10 parts Water 15 parts Sodium salicylate 1 part

XVI.—Soak 5 parts of Cologne glue in an aqueous calcium chloride solution (1:4) and heat on the water bath until dissolved, replacing the evaporating water; or slack 100 parts of lime with 150 parts of hot water, dissolve 60 parts of sugar in 180 parts of water, and add 15 parts of the slacked lime to the solution, heating the whole to 75° C. (167° F.). Place aside for a few days, shaking from time to time. In the clear sugar-lime solution collected by decanting soak 60 parts of glue and assist the solution by moderate heating.

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