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Some Experiments Concerning Mercury · Herman Boerhaave — chapter 5 of 7 · ~617 words · public domain

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EXPERIMENT VIII.

Further to examine the Powder remaining after the foregoing Operation.

The Operation.

Seven Drachms and 37 Grains of that Powder in a very clean Glass Retort, cased over with a Coat of Sand and Clay, I put into the naked Fire, which was carefully increased by Degrees, ’till the little Retort, which was entirely covered with the Coals, grew quite red hot. In this Degree of Heat I kept it for four Hours.

The Effect.

In the Receiver was seven Drams of most pure Mercury reviv’d from this Powder. In the Bottom of the Retort were 15 Grains of a dark, subtle, and fixed Powder, in so strong and lasting a Fire. There was a broad Spot, very thin, of a beautiful red, impressed on the Bottom of the Retort, and, as it were, penetrating into the Glass.

COROLLARIES.

1. Mercury by Fire alone is changed into the Powder above describ’d. (2, 4, 5, 6, 7, 8.)

2. This Powder, by Fire alone, but a stronger, is changed into Mercury.

3. Thus the Serpent that has bitten itself dies.

4. It arises again more glorious from Death.

5. So much Labour, and so great Fire being so long sustain’d, out of 17 Ounces of Mercury, only 15 Grains remain’d fix’d in the Glass, which was so hot, that it was ready to melt.

6. Silver, Gold, and other Metals fought for by this Art out of Quicksilver, is scarce any, in Proportion to the Charge and Labour.

7. Of the Powder so fix’d from Mercury, only the 72ᵈ Part remains fix’d in this Fire, the rest returns to Mercury.

8. Twenty-two Grains were lost. Were they dispers’d? or was this Quantity of Weight first accreted to the Mercury by Fire, thence again separated by a stronger Fire?

9. The Nature of Mercury is constant, simple, and cannot be separated into dissimilar Parts by Distillation; not into fix’d and volatile; not into pure and impure; not into feces and defecated; not into different Elements.

EXPERIMENT IX.

I put thirteen Grains of this last fix’d Powder (VIII.) into a Crucible, and set it over an open Fire before the Bellows: I increas’d the Heat of the Fire, by blowing till the whole Crucible was red hot: I kept it so for a Quarter of an Hour. The Powder remain’d fix’d in the Bottom, but swell’d up like a Spunge, and of a dark Colour. From hence I learn’d that this Powder had acquired a considerable Degree of Fixedness by Fire alone.

EXPERIMENT X.

Then I added to this fix’d Powder (IX.) some Borax in a Crucible, and increased the Fire by blowing. It became one Mass, brittle, growing like Glass, and fix’d in this great Fire.

EXPERIMENT XI.

I gave 2 Grains of that Powder, which had remained fix’d, to the Weight of 15 Grains (VIII.) to a sworn and very skilful Essayer of Metals at AMSTERDAM, to examine it with all possible Accuracy according to the Rules of Art, with Lead. Nothing fix’d remain’d: Therefore in that Powder there was not the least Gold or Silver.

EXPERIMENT XII.

The thirteen Grains melted down with the Borax into a Mass growing like Glass (almost vitrified) (X.) I gave to a sworn and very skilful Essayer of Metals at AMSTERDAM, to examine this whole little Mass with the greatest Accuracy, according to the Rules of Art, in Lead. Nothing fix’d remain’d of the whole Mass; so there was no Gold nor Silver in it.

COROLLARIES.

1. Quicksilver persists in the Fire, retaining its Nature unalterable.

2. Simple, and not separable, into different Parts by Distillation.

3. It is fixed by Fire, and seems changed in its outward Form.

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