Part 44

Introduction of the Microscope.

The beginnings of a particular branch of science are generally obscure and rooted so imperceptibly in the foundations on which it rests that it is difficult to point to any particular place in its development and say that this is the start. There are exceptions of course, like the remarkable work of Willard Gibbs in physical chemistry, and it may chance that the happy inspiration of a single worker may give such direction to methods of investigation as to open the gates into a whole new realm of research, and to thus create a separate scientific field, as happened in Radiochemistry.

This is what occurred in petrology when Sorby in England, in 1858, pointed out the value of the microscope as an instrument of research in geologic investigations, and demonstrated that its employment in the study of thin sections of rocks would yield information of the highest value. Others beside Sorby had made use of the microscope, as pointed out by Zirkel, but, as he indicates, no one before him had recognized its value. During the next ten years or so, however, its recognition was very slow and the papers published by Sorby himself were mainly concerned in settling very special matters.

As Williams has suggested, the greatest service of Sorby was, perhaps, his instructing Zirkel in his ideas and methods, for the latter threw himself whole-heartedly into the study of rocks by the aid of the microscope and his discoveries stimulated other workers in this field in Germany, his native country, until the dawning science of petrology began to assume form. A further step forward was taken in 1873 in the appearance of the text-books of Zirkel and Rosenbusch which collated the knowledge which had been gained and furnished the investigator more precise methods of work. It is difficult for the student of to-day to realize how much had been learned in the interval and, for that matter, how much has been gained since 1873, without an inspection of these now obsolete texts. In 1863, Zirkel, who was then at the beginning of his work, said in his first paper presented to the Vienna Academy of Sciences that if he confined himself chiefly to the structure of the rocks investigated and of their component minerals, and stated little as to what these minerals were, the reason for that was because “although the microscope serves splendidly for the investigation of the former relations, it promises very little help for the latter. Labradorite, oligoclase and orthoclase, augite and hornblende, minerals whose recognition offers the most important problems in petrography, in most cases cannot be distinguished from one another under the microscope.” How little could Zirkel have foreseen, at this time, less than forty years later, that not only could labradorite be accurately determined in a rock-section, but that in a few minutes by the making of two or three measurements on a properly selected section, its chemical composition and the crystallographic orientation of the section itself could be determined!

The Thin Section.

Before going further we may pause here a moment to consider the origin and development of the thin section, without which no progress could have been made in this field of research. When we reflect upon the matter, it seems a marvelous thing indeed that the densest, blackest rock can be made to yield a section of the ¹⁄₁₀₀₀ of an inch in thickness, so thin and transparent that fine printing can be easily read through it, and transmitting light so clearly that the most high-powered objectives of the microscope can be used to discern and study the minutest structures it presents with the same capacity that they can be employed upon sections of organic material prepared by the microtome. This is no small achievement.

The first thin sections appear to have been prepared in 1828 by William Nicol of Edinburgh, to whom we owe the prism which carries his name. He undertook the making of sections from fossil wood for the purpose of studying its structure. The method he developed was in principle the same as that employed to-day, where machinery is not used; that is, he ground a flat smooth surface upon one side of a chip of his petrified wood, then cemented this to a bit of glass plate with Canada balsam, and ground down the other side until the section was sufficiently thin. This method was used by others for the study of fossil woods, coal, etc., but it was not applied to rocks until 1850, when Sorby used it for investigating a calcareous grit. Oschatz, in Germany, also about this time independently discovered the same method. A further advance was made in melting the cement, floating off the slice, and transferring it to a suitable object-glass with cover, a process still employed by many; though most operators now cement the first prepared surface of the rock chip directly to the object-glass, and mount the section without transferring it.

Next came the use of machinery to save labor in grinding, and another step was made in the introduction of the saw, a circular disk of sheet iron whose edge was furnished with embedded diamond dust. This makes it possible to cut relatively thin slices with comparative rapidity, but the final grinding which requires experience and skill must still be done by hand. Carborundum has also largely replaced emery. The skill and technique of preparers has reached a point where sections of rocks of the desired thinness (0·001 inch), and four or five inches square have been exhibited.

The Era of Petrography.

In these earlier days of the science, as noted above, great difficulty was at first experienced in the recognition of the minerals as they were encountered in the study of rocks under the microscope. At that time the chemical composition and outward crystal form of minerals were relatively much better known than their physical and, especially, their optical properties and constants. Some beginnings in this had been made by Brewster, Nicol, and other physicists, and the mineralogists had commenced to study minerals from this viewpoint. Especially Des Cloiseaux had devoted himself to determining the optical properties of many minerals, and the writer, when a student in the laboratory of Rosenbusch in 1890, well recalls the tribute that he paid to the work of Des Cloiseaux for the aid which it had afforded him in his earlier researches in petrography.

The twenty years following the publication of the texts of Rosenbusch and Zirkel may be characterized as the era of microscopical petrography. A distinction is drawn here between the latter word and petrology, a distinction often overlooked, for petrography means literally the description of rocks, whereas petrology denotes the science of rocks. As time passed the broader and more fundamental features of rocks, especially of igneous and metamorphic rocks, in addition to their mineral constitution, were more studied and gained greater recognition, petrography gradually became a department of the larger field of petrology—the science of to-day.

The use of the microscope, as soon as the method became more generally understood, opened up so vast a field for investigation that at first the study and description of the rocks seemed of prime importance. This was natural, for hitherto the finer grained rocks had for the most part defied any adequate elucidation and here was a key which enabled one to read the cipher. A flood of literature upon the composition, structure, and other characters of rocks from all parts of the world began to appear in ever increasing volume. The demands of the petrographers for a greater and more accurate knowledge of the physical and optical constants of minerals stimulated this side of mineralogy, and increasing attention was given to investigations in this direction. No definite line between the two closely related sciences could be drawn, and a large part of the work published under the heading of petrography could perhaps be as well, or better, described under the title of micro-mineralogy. To some, in truth, the rocks presented themselves simply as aggregates of minerals, occurring in fine grains.

The work of the German petrographers attracted attention and drew students from all parts of the world to their laboratories, especially to those of Zirkel and Rosenbusch. The great opportunities, facilities, and freedom for work which the German universities had long offered to foreign students of science naturally encouraged this. In France a brilliant school of petrologists, under the able leadership of Michel-Lévy and Fouqué, had arisen whose work has been continued by Barrois, Lacroix and others, but the rigid structure of the French universities at that period did not permit of the offering of great inducements for the attendance of foreign students. The work of the French petrographers will be noticed in another connection.

In Great Britain, the home of Sorby, the new science progressed at first slowly, until it was taken up by Allport, Bonney, Judd, Rutley, and others. In 1885 the evidence of the advance that had been made and of the firm basis on which the new science was now placed appeared in Teall’s great work, “British Petrography,” which marked an epoch in that country in petrographic publication. This work was of importance also in another direction than that of descriptive petrography, in that it contains valuable suggestions for the application of the principles of modern physical chemistry in solving the problems of the origin of igneous rocks. In it, as in the publications of Lagorio, we see the passage of the petrographic into the petrologic phase of the science.

The earliest publication in America of the results of microscopic investigation of rocks that the writer has been able to find is by A. A. Julien and C. E. Wright, chiefly on greenstones and chloritic schists from the iron-bearing regions of upper Michigan. Naturally, it was of a brief and elementary character. In 1874 E. S. Dana read a paper before the American Association for the Advancement of Science on the result of his studies on the “Trap-rocks of the Connecticut valley,” an abstract of which was published in this Journal. Meanwhile Clarence King, in charge of the 40th Parallel survey, feeling the need of a systematic study of the crystalline rocks which had been encountered, and finding no one in this country prepared to undertake it, had induced Zirkel to give his attention to this task. The result of this labor appeared in 1876 in a fine volume which attracted great attention. In the same year appeared also petrographical papers by J. H. Caswell, E. S. Dana and G. W. Hawes. The latter devoted himself almost entirely to this field of research and may thus, perhaps, be termed the earliest of the petrographers in this country. His work, “The Mineralogy and Lithology of New Hampshire,” issued in 1878 as one of the reports of the State Survey under Prof. C. H. Hitchcock, was the first considerable memoir by an American. This was followed by various papers, one on the “Albany Granite and its contact phenomena,” being of especial interest as one of the earliest studies of a contact zone, and in the fullness of methods employed in attacking the problem forecasting the change to the petrology era.

During the ten years following, or from 1880 to 1890, the new science of petrography flourished and grew exceedingly. Many young geologists abroad devoted themselves to this field of research and the store of accumulated knowledge concerning rocks from all parts of the world, and their relations grew apace. The work of Teall has been noticed and among others might be mentioned the name of Brögger, whose first contribution in this field gave evidence that his publications would become classics in the science.

In America there appeared in this period a number of eager workers, trained in part in the laboratories of Rosenbusch and Zirkel, whose researches were destined to place the science on the secure footing in this country which it occupies to-day. Among the earlier of these may be mentioned Whitman Cross, R. D. Irving, J. P. Iddings, G. H. Williams, J. F. Kemp, J. S. Diller, B. K. Emerson, M. E. Wadsworth, G. P. Merrill, N. H. Winchell, and F. D. Adams in Canada. Others were added yearly to this group. As a result of their work a constantly growing volume of information about the rocks of America became available, and one has only to examine the files of the Journal and other periodicals and the listed publications of the National and State Surveys to appreciate this.

In the Journal, for example, we may refer to papers by Emerson on the Deerfield dike and its minerals, and on the occurrence of nephelite syenite at Beemersville, N. J.; to various interesting articles by Cross on lavas from Colorado and the pneumatolytic and other minerals associated with them; to important papers by Iddings on the rocks of the volcanoes of the Northwest, and those of the Great Basin, to primary quartz in basalt, and the origin of lithophysæ; to the results of researches by G. H. Williams on the rocks of the Cortlandt series, and on peridotite near Syracuse, N. Y.; to papers by Diller on the peridotites of Kentucky, and recent volcanic eruptions in California; to articles by R. D. Irving on the copper-bearing and other rocks of the Lake Superior region, and to Kemp on dikes and other eruptives in southern New York and northern New Jersey. Other publications would greatly extend this list.

The Petrologic Era.

As the chief facts regarding rocks, especially igneous rocks, as to their mineral and chemical composition, their structure and texture and the limits within which these are enclosed, became better known; and the relations, which these bear to the associations of rocks and their modes of occurrence, began to be perceived, the science assumed a broader aspect. The perception that rocks were no longer to be regarded merely as interesting assemblages of minerals, but as entities whose characters and associations had a meaning, increased. More and better rock analyses stimulated interest on the chemical side and this and the genesis of their minerals led to a consideration of the magmas and their functions in rock-making. The fact that the different kinds of rocks were not scattered indiscriminately, but that different regions exhibited certain groupings with common characters, was noticed. These features led to attempts to classify igneous rocks on different lines from those hitherto employed, and to account for their origin on broad principles. In other words, the descriptive science of petrography merged into the broader one of petrology. No exact time can be set which marks this passage, since the evolution was gradual. Yet for this country, in reviewing the literature, for which the successive issues of the “Bibliography of North American Geology” published by the U. S. Geological Survey has been of the greatest value; the writer has been struck by the fact that in the first volume containing the index of papers down to and including 1891, the articles on subjects of this nature are listed under the heading of petrography, whereas in the second volume (1892–1900) they are grouped under petrology and the former heading is omitted. A justification for this is found in examining the list of publications and noting their character. With some reason, therefore, the beginning of this period may be placed as in the early years of this decade. Furthermore, it was at this time that the great work of Zirkel began to appear, which sums up so completely the results of the petrographic era. Rosenbusch was formulating more definitely his views on the division of rocks into magmatic groups, as displayed by their associations in the field, and using this in classification; an idea which, appearing first in the second edition of his “Physiographie der massigen Gesteine,” finds fuller development in the third and last editions of this work. In this country Iddings published an important paper, in which the family relationships of igneous rocks and the derivation of diverse groups from a common magma by differentiation are clearly brought out. The fundamental problems underlying the genesis of igneous rocks had now been clearly recognized, and with this recognition the science passed into the petrologic phase. Brögger also had ascribed to the alkalic rocks of South Norway a common parentage and had pointed out their regional peculiarities.

From this time forward an attempt may be noted to find an analogy between rocks and the forms of organic life and to apply those principles of evolution and descent, which have proved so fruitful in the advancement of the biological sciences, to the genesis and classification of igneous rocks. This, perhaps, has on the whole been more apparent than real, in the constant borrowing of terms from those sciences to express certain features and relationships observed, or imagined, to obtain among rocks. Nevertheless, the perception of certain relations which we owe so largely to Rosenbusch and to Brögger has proved of undoubted value in furnishing a stimulus for the investigation of new regions, and in affording indications of what the petrologist should anticipate in his work.

Thus, the labors of the men previously mentioned, with those of Bayley, Bascom, Cushing, Daly, Lane, Lawson, Lindgren, Pirsson, J. F. Williams, Washington, and others, have thrown a flood of light upon the igneous rocks of this continent, and has made it possible to draw many broad generalizations concerning their origin and distribution. Thus, the differentiated laccoliths of Montana have been of service in affording clear examples of the process of local differentiation. Many papers published in the Journal during the last twenty years show this evolution and growth of petrological ideas. The contributions from American sources during this later period, and of which those in the Journal form a considerable fraction, have indeed been of great weight in shaping the development and future of the science.

By referring to the files of the Journal, it will be seen that they cover a continually widening range of subjects concerning rocks, and articles of theoretical interest are more and more in evidence, along with those of a purely descriptive character. Thus we find discussions by Becker on the physical constants of rocks, on fractional crystallization, and on differentiation; by Cross on classification; by Adams on the physical properties of rocks; by Daly on the methods of igneous intrusion; by Wright on schistosity; by Fenner on the crystallization of basaltic magma; by Bowen on differentiation by crystallization; by the writer on complementary rocks and on the origin of phenocrysts; by Smyth on the origin of alkalic rocks; by Murgoci on the genesis of riebeckite rocks; and by Barrell on contact-metamorphism. These may serve as examples, selected almost at random, from the files of the Journal, and we find with them articles descriptive of the petrology of many particular regions, which often contain also matter of general interest and importance, such as papers by Lindgren on the granodiorite and related rocks of the Sierra Nevada; by Ransome on latite; by Cross on the Leucite Hills; by Hague on the lavas of the Yellowstone Park; by Pogue on ancient volcanic rocks from North Carolina; by Warren on peridotites from Cumberland, R. I.; on sandstone from Texas by Goldman; and on the petrology of various localities in central New Hampshire by Washington and the writer. Such a list could of course be much extended and other papers of importance be cited, but enough has been said to indicate how important a repository of the results of petrologic research the Journal has been and continues to be.

In thus looking backward over the list of active workers we are involuntarily led to pause and reflect how great a loss American petrology has sustained in the premature death of some of its most brilliant and promising exponents; it is only necessary to recall the names of R. D. Irving, G. H. Williams, G. W. Hawes, J. F. Williams and Carville Lewis, to appreciate this.

The store of material gathered during these years has led to the publication of extensive memoirs, in which the science is treated not from the older descriptive side, but from the theoretical standpoint and of classification. In these works strong divergencies of views and opinions are observed, which is a healthy sign in a developing science.

It should be also noted that along with this evolution on the theoretical side there has been a constant improvement in the technique of investigating rocks. It is only necessary to compare the older handbooks of Zirkel and Rosenbusch with the many modern treatises on petrographic methods to be assured of this. It is due on the one hand to the vast amount of careful work which has been done in accurately determining the physical constants of rock-minerals and in arranging these for their determination microscopically, as in the remarkable studies on the feldspars by Michel-Lévy, and on the other in researches on the apparatus employed, and in consequent improvements in them and in ways of using them, as exemplified in the delicately accurate methods introduced by Wright. The development of the microscope itself as an instrument of research in this field and in mineralogy deserves a further word in this connection. The first step toward making the ordinary microscope of special use in this way was taken by Henry Fox Talbot of England, when he introduced in 1834 the employment of the recently invented nicol prisms for testing objects in polarized light. The modern instrument may be said to date from the design offered by Rosenbusch in 1876. Since that time there have been constant improvements, almost year by year, until the instrument has become one of great precision and convenience, remarkably well adapted for the work it is called upon to perform, with special designs for various kinds of use, and an almost endless number of accessory appliances for research in different branches of mineralogy and crystallography, as well as in petrography proper. This also calls to mind the fact that for the convenience of those who are not able to use the microscope special manuals of petrology have been prepared in which rocks are treated from the megascopic standpoint.

Metamorphic Rocks.

In this connection the metamorphic rocks should not be forgotten. They afford indeed the most difficult problems with which the geologist has to deal; every branch of geological science may in turn be called upon to furnish its quota for help in solving them. Under the attack of careful, accurate and persistent work in the field, under the microscope and in the chemical laboratory, with the aid of the garnered knowledge in petrology, stratigraphy, physiography, and other fields of geologic science, their mystery has in large part given way. The inaugural work of Lehmann, Lossen, Barrois, Bonney, Teall, and other European geologists, was paralleled in America by that of R. D. Irving, owing to whose efforts the Lake Superior region became the chief place of study of the metamorphic rocks in this country. Irving soon obtained the assistance of G. H. Williams, who had been engaged in the study of such rocks, and the latter published a memoir on the greenstone schist areas of Menominee and Marquette in Michigan which will always remain one of the classics in the literature of metamorphic rocks. Irving’s own contributions to petrology, though valuable, were cut short by his untimely death, but the study of this region under the direction of his associate and successor, C. R. Van Hise, with his co-laborers, has yielded a mass of information of fundamental importance in our understanding of metamorphism and the crystalline schists. Its fruitage appears in the memoir by Van Hise which is the authoritative work of reference on metamorphism, and in various publications by him and his assistants, Bayley, Clements, Leith, and others. The work of the Canadian geologists, and of Kemp, Cushing, Smyth and Miller in the Adirondack region, should also be mentioned in connection with this field of petrology.